【公開日：2024.07.25】【最終更新日：2024.06.29】
課題データ / Project Data
課題番号 / Project Issue Number
23UT0372
利用課題名 / Title
Structural analysis of MOF crystals
利用した実施機関 / Support Institute
東京大学 / Tokyo Univ.
機関外・機関内の利用 / External or Internal Use
内部利用（ARIM事業参画者以外）/Internal Use (by non ARIM members)
技術領域 / Technology Area
【横断技術領域 / Cross-Technology Area】（主 / Main）計測・分析/Advanced Characterization（副 / Sub）-
【重要技術領域 / Important Technology Area】（主 / Main）次世代ナノスケールマテリアル/Next-generation nanoscale materials（副 / Sub）-
キーワード / Keywords
X線回折/ X-ray diffraction,ナノ多孔体/ Nanoporuous material
利用者と利用形態 / User and Support Type
利用者名（課題申請者）/ User Name (Project Applicant)
FU Jiarui
所属名 / Affiliation
東京大学 大学院理学系研究科
共同利用者氏名 / Names of Collaborators in Other Institutes Than Hub and Spoke Institutes
ARIM実施機関支援担当者 / Names of Collaborators in The Hub and Spoke Institutes
利用形態 / Support Type
（主 / Main）機器利用/Equipment Utilization（副 / Sub）-
利用した主な設備 / Equipment Used in This Project
報告書データ / Report
概要（目的・用途・実施内容）/ Abstract (Aim, Use Applications and Contents)
These measurements are qualitative X-ray analyses for crystals. I prepared four crystals and I wanted to know the phase and crystallinity. The samples are 300-1000 nm powder crystals. They are metal-organic framework crystals. My purpose is to use the fast scan of XRD (SmartLab (Kα1)) to screen samples.
実験 / Experimental
I prepared a few mg scale samples for each test. The 2 Theta ranged from 5 degrees to 40 degrees because the crystal had large lattice parameters. Due to the fast scanning and good crystallinity, testing all samples requires less than 2 hours.
結果と考察 / Results and Discussion
In my research, I have meticulously assessed the crystallinity of four distinct metal-organic crystals, each demonstrating commendable structural integrity and potential for further exploration. Following a thorough evaluation, I have elected to focus on one particular metal-organic crystal for future in-depth study and analysis.This decision was informed by a comprehensive consideration of various factors, including the crystal's structural properties, its compatibility with the electron irradiation technique utilized in my research, and its potential applicability in the development of glass materials with enhanced sustainability and functionality.The selected metal-organic crystal exhibits promising characteristics that render it exceptionally well-suited for comprehensive investigation. Its robust crystalline structure presents an ideal platform for probing the intricate relationships between structure and properties, shedding light on its behavior under electron irradiation and providing valuable insights into its suitability as a precursor for hybrid metal-organic glass materials.By leveraging the unique properties and versatility of this metal-organic crystal, I aim to delve deeper into its molecular architecture, elucidating its response to electron bombardment and elucidating the underlying mechanisms governing its synthesis and properties. This endeavor holds significant promise for advancing our understanding of metal-organic glasses and unlocking their full potential in sustainable materials design and manufacturing.Furthermore, by focusing on the development of environmentally friendly glass materials with tailored functionalities, my research aligns closely with the principles of green transformation (GX). By advancing sustainable manufacturing practices and fostering the creation of novel materials with reduced environmental impact, we can contribute to building a more resilient and environmentally conscious future for generations to come. Through rigorous experimentation, analysis, and innovation, we can pave the way for the emergence of a new generation of glass materials that not only meet the demands of modern society but also safeguard the health and well-being of our planet.
図・表・数式 / Figures, Tables and Equations
その他・特記事項（参考文献・謝辞等） / Remarks(References and Acknowledgements)
成果発表・成果利用 / Publication and Patents
論文・プロシーディング（DOIのあるもの） / DOI (Publication and Proceedings)
口頭発表、ポスター発表および、その他の論文 / Oral Presentations etc.
特許 / Patents
特許出願件数 / Number of Patent Applications：0件
特許登録件数 / Number of Registered Patents：0件