利用報告書 / User's Reports


【公開日:2023.07.31】【最終更新日:2023.05.17】

課題データ / Project Data

課題番号 / Project Issue Number

22UT0378

利用課題名 / Title

Material Assessment for Liquified Hydrogen Storage Tank

利用した実施機関 / Support Institute

東京大学 / Tokyo Univ.

機関外・機関内の利用 / External or Internal Use

内部利用(ARIM事業参画者以外)/Internal Use (by non ARIM members)

技術領域 / Technology Area

【横断技術領域 / Cross-Technology Area】(主 / Main)計測・分析/Advanced Characterization(副 / Sub)-

【重要技術領域 / Important Technology Area】(主 / Main)革新的なエネルギー変換を可能とするマテリアル/Materials enabling innovative energy conversion(副 / Sub)-

キーワード / Keywords

SUS316L stainless steel, EBSD,電子顕微鏡/Electron microscopy,電子顕微鏡/Electron microscopy


利用者と利用形態 / User and Support Type

利用者名(課題申請者)/ User Name (Project Applicant)

Magalhaes de Melo Freire Rafael

所属名 / Affiliation

東京大学

共同利用者氏名 / Names of Collaborators in Other Institutes Than Hub and Spoke Institutes

Tomoya Kawabata,Mitsuo Kimura

ARIM実施機関支援担当者 / Names of Collaborators in The Hub and Spoke Institutes
利用形態 / Support Type

(主 / Main)機器利用/Equipment Utilization(副 / Sub)-


利用した主な設備 / Equipment Used in This Project

UT-103:高分解能走査型電子顕微鏡


報告書データ / Report

概要(目的・用途・実施内容)/ Abstract (Aim, Use Applications and Contents)

To investigate the properties and mechanism of failure of SUS316L stainless steel, a fracture tensile specimen was cut in the longitudinal direction to be observed by EBSD. The polishing of the EBSD sample was carried out in the Kawabata's Laboratory at the University of Tokyo and the EBSD observation was conducted at Advanced Research Infrastructure for Materials and Nanotechnology in Japan. This work consisted of an attempt to characterize the material and learn the basic concepts of EBSD.

実験 / Experimental

First, the quality of polishing procedure was accessed by SEM images and it was acceptable. The cleaning procedure of the sample was indicated as one possible point to improve in order to obtain better images.
Then, EBSD analysis was executed with one tensile fractured specimen. 

結果と考察 / Results and Discussion

From the images obtained by EBSD, it was difficult to describe the failure mechanism since the image quality was affected by the high strain level. The experiment was useful to understand the difficult task in characterize a material that failed in ductile mode with high strain levels. Methods and strategies to deal with this issue can be adopted from this trial experiment at ARIM.

図・表・数式 / Figures, Tables and Equations
その他・特記事項(参考文献・謝辞等) / Remarks(References and Acknowledgements)

We thank Fukukawa San for the teaching and support in English about how to use the machine. We also thank the administrative team from ARIM for taking care of the communication and schedule for the experiment.


成果発表・成果利用 / Publication and Patents

論文・プロシーディング(DOIのあるもの) / DOI (Publication and Proceedings)
口頭発表、ポスター発表および、その他の論文 / Oral Presentations etc.
特許 / Patents

特許出願件数 / Number of Patent Applications:0件
特許登録件数 / Number of Registered Patents:0件

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